Method 8270 5 point curve w/o ISTD's

2,4-Dinitrophenol, 4-Nitrophenol, and Pentachlorophenol are susceptible to adsorption on active surfaces found in injection ports or contaminated columns.
We have found that benzidine degrades in multi-component semi-volatile solutions. Therefore the benzidine in any calibration curve should be used as a qualitative retention time marker. Reported hits for benzidine should be quantitatively determined by analyzing a single benzidine solution or by using the benzidine response observed in the Daily GC/MS tuning solution.